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Pioglitazone, is a medication prescribed for the treatment of type 2 diabetes. Pioglitazone was synthesized via a five step pathway, commencing from commercially available 1-fluoronitrobenzene Condensation of the latter with 2- 5-ethylpyridyl ethanol provided pyridylethoxybenzene that subsequently was hydrogenated using Pd on charcoal as catalyst to provide the anticipated aromatic amine The latter was subjected into cyclocondensation with thiourea, gave an imino compound as intermediate which upon hydrolysis provided the desired target pioglitazone Scheme Lansoprazole, which reduces stomach acid, was patented in and approved for medical use in This method was improved later and patented.

In principle, it is the synthetic route of omeprazole, only divergent in details and characteristics, for instance, instead of 2,3,5-collidine as a starting material, 2,3-lutidine was chosen, and the methoxy moiety in the fourth position of pyridine ring was changed by the 2,2,2-trifluoroethoxy moiety. Nifedipine is a famous medication used to regulate high blood pressure. It is also a calcium channel blocker of the dihydropyridine type.

Nifedipine was patented in and commercialized by Hofmann La Roch in under the trade name of Adalat among others. Amlodipine, is an approved drug used to treat high blood pressure and coronary artery disease. It is also presently sold under the brand name Norvasc. This name reaction involves a simple procedure and straightforward isolation of product. Amlodipine was synthesized as depicted in Scheme Next, the side chain at C-2 in amlodipine was successfully introduced via a procedure patented by Pfizer company.

It was found that only C-2 position was selectively brominated over C-6 position. At the end, reduction of azido group using zinc dust to amine was achieved to give the desired amlodipine in satisfactory yield. Rosuvastatin, is drug that inhibits the synthesis of cholesterol and promote the production of LDL-binding receptors in the liver. It was first patented in and marketed in under brand name of Crestor.

The sulfur scaffold in the resultant S -methyl pyrimidine was oxidized employing m -chloroperbenzoic acid m -CPBA in CHCl 3 to provide methylsulfonylpyrimidine Upon reduction of the ester group of the latter using diisobutylaluminium hydride DIBAL in toluene the corresponding primary alcohol was obtained which upon oxidation using tetrapropylammonium perruthenate TPAP provided the respective aldehyde At last the latter treated with aqueous sodium hydroxide to provide the respective sodium salt that was converted into desired calcium salt, rosuvastatin Scheme Azelastine is a medication which is primarily used as a nasal spray to treat allergic rhinitis hay fever.

It invoved the reaction of hydrazine with keto-acid to give phthalazinone The latter was reacted with 2- 2-chloroethyl - N -methylpyrrolidine in hot aqueous NaOH provided azelastine via a fascinating ring expansion. This ring expansion apparently proceeds via the intermediacy of 3. Notably, by using a solid hydrazide instead of volatile hydrazine this route is longer but it is a safer alternative at large scale production.

Hydralazine, is a medication used to treat high blood pressure and heart failure. The latter was reacted with hydrazine hydrate to give phthalazone, which upon treatment with phosphorous oxychloride to give 1-chloroph-thalazine In the last steps substitution of the chlorine atom with hydrazine affords the desired hydralazine Scheme Glipizide, is an anti-diabetic medication of the sulfonylurea class prescribed for the treatment of type 2 diabetes and is used combined with a diabetic diet.

It was approved for medical in and introduced to market under the brand name Glucotrol. As depicted in Scheme 44, the synthesis of glipizide, is started with 6-methylpyrazincarboxylic acid which is initially treated with SOCl 2, leading to the respective chloride that is further reacted with 4- 2-aminoethyl benzenesulfonamide, giving the expected amide Lamotrigine, came to market in the Great Britain in as is an anticonvulsant medication prescibed for treatment and epilepsy and bipolar disorder.

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